Titan ReloadingWidenersInline FabricationRepackbox
MidSouth Shooters SupplyRotoMetals2Snyders JerkyLoad Data
Lee Precision Reloading Everything

Thread: My homemade black powder

  1. #2021
    Boolit Master
    Join Date
    Apr 2010
    Posts
    2,287
    You let them dry for a day & see how hard they are then.

    Fly

  2. #2022
    Boolit Master

    Join Date
    Aug 2011
    Posts
    3,493
    I also get better pucks when it oozes some. Fine line indeed. Lots of oozing is a HUGE mess and lots of wastage. But not enough and my pucks fall apart into dust.

    The golden state is when it oozes clear liquid. That is a supreme fine line, but that magic land is super clean and results in excellent pucks.

  3. #2023
    Boolit Master
    Join Date
    Apr 2010
    Posts
    2,287
    I been doing this for some time & zero water comes out of mine. I have a friend in Florida who is the smartest
    man I know in making BP & fireworks. He makes commercial fire works for a living & taught me much, & written
    a few book on top of that. He tells me he does not even wet his because of the humidity in Fla.

    I don't know guys I have made countless puck dies & never had a complaint. I have not a clue what the problem is.
    Wish I could help.
    Fly

  4. #2024
    Boolit Buddy fishingsetx's Avatar
    Join Date
    Apr 2015
    Location
    silsbee, tx
    Posts
    203
    Quote Originally Posted by brian1 View Post
    I got my pucks made. They weighed 14.5 oz, so I apparently lost 1.5 oz in the process. Funny thing is, when I got it down to dry enough that it wasn't oozing much, it really didn't press quite as hard and tight as it did when it was oozing, even when I really cranked it up to max pressure. It seems the proper wetness is a very fine line. It seems like I got better pucks when it was wet enough to ooze some. Top 2 small pucks were from the first die version, top one from Die-II was after the mix got dried out, and the edges kinda flaked off. The rest I did at that dryness were done at max pressure on the 30 ton press.


    Attachment 217654
    Pic is kinda fuzzy, but a few of those look like some I made and didnt add enough water.

    How fine was your green mill?,

    I add just enough water to get the mill to start to try and cake togetger when pressed by hand. I use a set of lee powder dippers to measure it and once I find the right amount, I stick with that. The amount may change between batches/days. Using fly's die and a 6 ton press, I want to see a VERY slight bead of water at max pressure. Doing it this way, my pressed pucks come out if the press hard as a rock. Usually the top edge of the puck is soft (around the corner), but I just scrape that off back into my green mill and repress with the next batch. Once dry (overnight in a dehydrator), they sound like a ceramic disk when tapped with something metal.

    If you didnt spill a large amount of powder, something is definitly amiss! 1.5 oz converts to 650+ grains of powder (by weight). Plus, you added water which should have increased the final weight even more! You should have seen that somewhere!

    Guns have only two enemies: rust and politicians!

  5. #2025
    Boolit Man brian1's Avatar
    Join Date
    Oct 2014
    Location
    NH
    Posts
    91
    Quote Originally Posted by fishingsetx View Post
    Pic is kinda fuzzy, but a few of those look like some I made and didnt add enough water.

    How fine was your green mill?,
    Yeah, it seemed like it acted like a bit too dry, yet I still got a small amount of clear water from it; as opposed to the much larger amounts of thick black goo I got when it was wetter. I just checked them, though - even the ones that looked like they might have been a bit dry are all quite hard. When I was pressing them, I gave them extra pressure, to make up for the dryness. The dryer ones aren't as glassy smooth on the non-piston side as the wetter ones were, but they are all quite hard.

    Quote Originally Posted by fishingsetx View Post
    If you didnt spill a large amount of powder, something is definitly amiss! 1.5 oz converts to 650+ grains of powder (by weight). Plus, you added water which should have increased the final weight even more! You should have seen that somewhere!
    At first, when I was getting more goo from it, I used my finger to scrape up the goo and put it back into the mixture. Later on, I was getting less goo and getting tired of the process (press puck, clean up goo, press out piston, clean packed mix from piston and cylinder, go remove the galling from piston and cylinder, etc), so I just wiped off anything coming out with a paper towel and threw it in the trash. For the last couple pucks, I went back to putting a thin layer of anti-seize on the piston wall, and that seemed to help with preventing galling.

    I wonder if temperatures have anything to do with all this. It's still below freezing here, especially at night. In fact, it's SNOWING right now!

  6. #2026
    Boolit Man brian1's Avatar
    Join Date
    Oct 2014
    Location
    NH
    Posts
    91
    Quote Originally Posted by Fly View Post
    I been doing this for some time & zero water comes out of mine. I have a friend in Florida who is the smartest
    man I know in making BP & fireworks. He makes commercial fire works for a living & taught me much, & written
    a few book on top of that. He tells me he does not even wet his because of the humidity in Fla.

    I don't know guys I have made countless puck dies & never had a complaint. I have not a clue what the problem is.
    Wish I could help.
    Fly
    One assumption I've been making is that your dies are aluminum. That's what I used. Perhaps you are using stainless steel. or are yours aluminum?

  7. #2027
    Boolit Buddy fishingsetx's Avatar
    Join Date
    Apr 2015
    Location
    silsbee, tx
    Posts
    203
    Quote Originally Posted by brian1 View Post
    One assumption I've been making is that your dies are aluminum. That's what I used. Perhaps you are using stainless steel. or are yours aluminum?
    Mine I got from him is aluminum. I do set the die on a piece of PTFE on the non piston side to try and seal it. My pucks come out slick and shiny everywhere except the corners. Id be leery of using neversieze for fear of powder contamination. Never had an issue with my die trying to sieze up. Not sure what the clearances between the barrel and piston are, compared to yours, though.

    How did you go about mixing the water in? The little bit of water (a couple tiny drops) that comes out when I press is almost black, but the consistancy of plain water.

    Guns have only two enemies: rust and politicians!

  8. #2028
    Boolit Man brian1's Avatar
    Join Date
    Oct 2014
    Location
    NH
    Posts
    91
    I used the anti-seize sparingly and only on the piston walls, so it should not be making any contact with the puck

    I just poured a small amount of distilled water in from a bottle, mixed with gloved hands until fully dispersed, then added a bit more & repeated until it seemed the moisture had gotten to all of it. I think another time it might be better to under-water, then let it sit a day or 2 covered, to let the water disperse that way, rather than trying to do it all at once.

    Perhaps next time I should put the die onto a piece of plastic (I have PVC boards), too. I was using a little 4" square of sheet aluminum to set between the bottom of the die and the press base.

  9. #2029
    Boolit Buddy Faret's Avatar
    Join Date
    Jan 2009
    Location
    South Central Wisconsin
    Posts
    472
    Every time I pressed mine I used 4% by weight distilled water and had just a slight amount of seepage of water. One could always use less say 3 or 3.5%?

  10. #2030
    Boolit Master
    swamp's Avatar
    Join Date
    Mar 2010
    Location
    Denver, CO
    Posts
    1,162
    I second the spritzer bottle. I use 91% alcohol in mine.
    swamp
    There is no problem so great, that it cannot be solved by the proper application of high explosives.

  11. #2031
    Boolit Man brian1's Avatar
    Join Date
    Oct 2014
    Location
    NH
    Posts
    91
    Very helpful advice there, swamp & indian joe - I will do it that way next time

  12. #2032
    Boolit Buddy
    Join Date
    Jul 2012
    Posts
    245
    Well, I made some more grinding media. I have a full tub full so I figure I now have enough, as I can fill each of the 2 tubs half-full of media:



    About all I need to do now is assemble my 12-ton Harbor Freight press.

    Steve

  13. #2033
    Boolit Master
    Join Date
    Apr 2010
    Posts
    2,287
    Man I love the way you roll those edges on those tubes.

    Fly

  14. #2034
    Boolit Buddy fishingsetx's Avatar
    Join Date
    Apr 2015
    Location
    silsbee, tx
    Posts
    203
    Quote Originally Posted by Fly View Post
    Man I love the way you roll those edges on those tubes.

    Fly
    Edit: went back and found his other post about how he does them. Much better than my dull cutter blade!

    Guns have only two enemies: rust and politicians!
    Last edited by fishingsetx; 04-08-2018 at 07:39 PM.

  15. #2035
    Boolit Master
    Join Date
    Jul 2013
    Location
    Florida
    Posts
    843
    I just started a batch and to my surprise the potassium nitrate has picked up a little moisture from the air. I'm milling it as usual but am wondering what will happen with the batch, will it mix properly or not. I'm planning to giving it a longer milling and will add some dextrin tomorrow before a final milling and then corning. Think the damp potassium nitrate will cause any problems?

  16. #2036
    Boolit Buddy fishingsetx's Avatar
    Join Date
    Apr 2015
    Location
    silsbee, tx
    Posts
    203
    I would say no, but that is just an educated guess. I cant see any reason a little moisture would effect it considering you will be adding more water to corn it (im assuming you dont press it into pucks).

    Guns have only two enemies: rust and politicians!

  17. #2037
    Boolit Master
    Join Date
    Jul 2013
    Location
    Florida
    Posts
    843
    The little bit of moisture didn't affect anything during the milling. Checked it and it looked good.

  18. #2038
    Boolit Master
    Join Date
    Apr 2010
    Posts
    2,287
    Eddie no need for a binder when Corning pressed powder.

    Fly

  19. #2039
    Boolit Master
    Join Date
    Jul 2013
    Location
    Florida
    Posts
    843
    Fly, I'm having trouble getting enough pressure with my press setup, the pucks are coming out soft. I'm going to try adding dextrin to get a better uniform grain size.

  20. #2040
    Boolit Master
    Join Date
    Apr 2010
    Posts
    2,287
    Ed how many ton press do you have.

    Fly

Page 102 of 410 FirstFirst ... 2529293949596979899100101102103104105106107108109110111112152202 ... LastLast

Posting Permissions

  • You may not post new threads
  • You may not post replies
  • You may not post attachments
  • You may not edit your posts
  •  
Abbreviations used in Reloading

BP Bronze Point IMR Improved Military Rifle PTD Pointed
BR Bench Rest M Magnum RN Round Nose
BT Boat Tail PL Power-Lokt SP Soft Point
C Compressed Charge PR Primer SPCL Soft Point "Core-Lokt"
HP Hollow Point PSPCL Pointed Soft Point "Core Lokt" C.O.L. Cartridge Overall Length
PSP Pointed Soft Point Spz Spitzer Point SBT Spitzer Boat Tail
LRN Lead Round Nose LWC Lead Wad Cutter LSWC Lead Semi Wad Cutter
GC Gas Check